A Multi-Analytical Approach for the Evaluation of the Efficiency of the Conservation-Restoration Treatment of Moroccan Historical Manuscripts Dating to the 16th, 17th, and 18th Centuries.
Identifieur interne : 000285 ( Main/Exploration ); précédent : 000284; suivant : 000286A Multi-Analytical Approach for the Evaluation of the Efficiency of the Conservation-Restoration Treatment of Moroccan Historical Manuscripts Dating to the 16th, 17th, and 18th Centuries.
Auteurs : Latifa Hajji ; Abdellatif Boukir ; Jamal Assouik ; Abdelali Kerbal ; Mohamed Kajjout ; Pierre Doumenq ; Maria Luisa De CarvalhoSource :
- Applied spectroscopy [ 1943-3530 ] ; 2015.
Abstract
The most critical steps during the conservation-restoration treatment applied in Moroccan libraries are the deacidification using immersion in a saturated aqueous calcium hydroxide (Ca(OH)2) solution and the consolidation of degraded manuscripts using Japanese paper. The present study aims to assess the efficiency of this restoration method using a multi-analytical approach. For this purpose, three ancient Arabic Moroccan manuscript papers dating back to the 16th, 17th, and 18th centuries were investigated to characterize the paper support and make a comparative study between pre-restoration and post-restoration states. Three structural and molecular characterization techniques including solid-state nuclear magnetic resonance spectroscopy on (13)C with cross-polarization and magic-angle spinning nuclear magnetic resonance ((13)C CP-MAS NMR), attenuated total reflectance Fourier transform infrared spectroscopy (ATR FT-IR), and X-ray diffraction (XRD) were used to elucidate the cellulose main features, to identify the inorganic composition of the papers, and to study the crystallinity of the samples. Inductively coupled plasma atomic emission spectrometry (ICP-AES) allowed us to obtain a qualitative and quantitative characterization of the mineral fillers used in the manufacturing of the papers. Scanning electron microscopy coupled to energy dispersive spectrometry (SEM-EDS) ascertained the state of conservation of the different papers and helped us to study the elemental composition of the samples. After restoration, it was shown that the deacidification improved the stability of papers by providing an important alkaline buffer, as demonstrated using FT-IR and energy dispersive spectrometry (EDS) results. However, XRD and ICP-AES did not confirm the pertinence of the treatment for all samples because of the unequal distribution of Ca on the paper surface during the restoration. The consolidation process was studied using SEM analysis; its effectiveness in restoring torn areas was found to be significant.
DOI: 10.1366/14-07688
PubMed: 26162347
Affiliations:
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The present study aims to assess the efficiency of this restoration method using a multi-analytical approach. For this purpose, three ancient Arabic Moroccan manuscript papers dating back to the 16th, 17th, and 18th centuries were investigated to characterize the paper support and make a comparative study between pre-restoration and post-restoration states. Three structural and molecular characterization techniques including solid-state nuclear magnetic resonance spectroscopy on (13)C with cross-polarization and magic-angle spinning nuclear magnetic resonance ((13)C CP-MAS NMR), attenuated total reflectance Fourier transform infrared spectroscopy (ATR FT-IR), and X-ray diffraction (XRD) were used to elucidate the cellulose main features, to identify the inorganic composition of the papers, and to study the crystallinity of the samples. Inductively coupled plasma atomic emission spectrometry (ICP-AES) allowed us to obtain a qualitative and quantitative characterization of the mineral fillers used in the manufacturing of the papers. Scanning electron microscopy coupled to energy dispersive spectrometry (SEM-EDS) ascertained the state of conservation of the different papers and helped us to study the elemental composition of the samples. After restoration, it was shown that the deacidification improved the stability of papers by providing an important alkaline buffer, as demonstrated using FT-IR and energy dispersive spectrometry (EDS) results. However, XRD and ICP-AES did not confirm the pertinence of the treatment for all samples because of the unequal distribution of Ca on the paper surface during the restoration. The consolidation process was studied using SEM analysis; its effectiveness in restoring torn areas was found to be significant. </div></front></TEI><affiliations><list></list><tree><noCountry><name sortKey="Assouik, Jamal" sort="Assouik, Jamal" uniqKey="Assouik J" first="Jamal" last="Assouik">Jamal Assouik</name><name sortKey="Boukir, Abdellatif" sort="Boukir, Abdellatif" uniqKey="Boukir A" first="Abdellatif" last="Boukir">Abdellatif Boukir</name><name sortKey="De Carvalho, Maria Luisa" sort="De Carvalho, Maria Luisa" uniqKey="De Carvalho M" first="Maria Luisa" last="De Carvalho">Maria Luisa De Carvalho</name><name sortKey="Doumenq, Pierre" sort="Doumenq, Pierre" uniqKey="Doumenq P" first="Pierre" last="Doumenq">Pierre Doumenq</name><name sortKey="Hajji, Latifa" sort="Hajji, Latifa" uniqKey="Hajji L" first="Latifa" last="Hajji">Latifa Hajji</name><name sortKey="Kajjout, Mohamed" sort="Kajjout, Mohamed" uniqKey="Kajjout M" first="Mohamed" last="Kajjout">Mohamed Kajjout</name><name sortKey="Kerbal, Abdelali" sort="Kerbal, Abdelali" uniqKey="Kerbal A" first="Abdelali" last="Kerbal">Abdelali Kerbal</name></noCountry></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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